(7aS)-(–)-Dimethyl(1-oxido-3-oxo-5,6,7,7a-tetrahydro-3H-pyrrolizin-2-yl)sulfonium

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(7aS)-(–)-Dimeth­yl(1-oxido-3-oxo-5,6,7,7a-tetra­hydro-3H-pyrrolizin-2-yl)sulfonium

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{2-[(Benzo­yloxy)meth­yl]-1-oxo-3H-pyrrolizin-2-yl}methyl benzoate

The title compound, C(23)H(19)NO(5), was prepared by esterification of 2,2-bis-(hy-droxy-meth-yl)-2,3-dihydro-1H-pyrrolizin-1-one with benzoyl chloride in pyridine·The pyrrolizine ring system is approximately planar with a maximum deviation of 0.008 (2) Å from the least-squares plane; the two phenyl rings are oriented at dihedral angles of 64.26 (11) and 70.75 (10)° with respect to the pyrroliz...

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(1S,2R,6R,7aS)-1,2,6-Trihy­droxy­hexa­hydro-1H-pyrrolizin-3-one

In the title compound, C(7)H(11)NO(4), prepared via a Morita-Baylis-Hillman adduct, the five-membered ring bearing three O atoms approximates to a twisted conformation, whereas the other ring is close to an envelope, with a C atom in the flap position. The dihedral angle between their mean planes (all atoms) is 23.11 (9)°. The new stereocenters are created in a trans-diaxial configuration. In t...

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Poly[[2-(3-pyridinio)-1H,3H +-benzimidazolium] [μ4-oxido-di-μ3-oxido-tetra-μ2-oxido-hexa­oxidotetra­molybdenum(VI)]]

The reaction of MoO(3) with 2-(3-pyrid-yl)benzoimidazole and water in the presence of MnSO(4)·5H(2)O at 453 K under hydro-thermal conditions afforded the title compound, {(C(12)H(11)N(2))[Mo(4)O(13)]}(n), in which infinite molybdenum oxide anionic chains are charge-balanced by diprotonated 2-(3-pyrid-yl)benzoimidazole (H(2)3-PBIM(2+)) cations. Eight [MoO(6)] octa-hedra are edge-shared, forming ...

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Ethyl 3-oxo-3H-benzo[f]chromene-2-carboxyl­ate

In the title compound, C(16)H(12)O(4), the chromene ring system is almost planar [maximum deviation = 0.026 (1) Å] and makes dihedral angles of 1.24 (9) and 26.5 (2)° with the fused benzene ring and the plane of the ethyl carboxyl-ate group, respectively.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2012

ISSN: 1600-5368

DOI: 10.1107/s1600536812003601